Shimadzu
Nexera
10년
주장비
분석
화합물 전처리·분석장비 > 분리분석장비 > 액체크로마토그래피
공동활용서비스
2022-08-31
62,319,520원
기관의뢰 직접사용
고정형
시간별
[Hr] 10,000원
본 장비는 검출부에 질량분석기를 사용하는 분석장비로서, 특정 화합물의 정성 및 정량분석을 수행하여 화학분석의 효율성을 제고해주는 장비. 체외진단 의료기기의 품질관리 중 항체 단백질의 확인시험, 순도시험 등 시험 진행에 필요
장비 구성 및 성능(Configurations and Specification)
1. System Controller(주장비)
1) User interface : Can be controlled via the PC browser or Touch Panel
2) Number of connectable units : 8(Option use 12)
3) Data buffering : Protects data being acquired even if the PC fails.
Up to 24 hours for one analysis, at 500ms sampling rate.
4) Event input/output : 1 inputs, 2 outputs
5) Analog board : up to two channel(option)
6) Network control : Can be networked using Ethernet connections.
2. Solvent delivery system(주장비)
1) Pumping Method : Parallel-type double plunger pump (approx. 10uL/1 stroke)
2) Flow Rate Setting Range : 0.0001 - 3.0000 mL/min(1.0 - 70 MPa), 3.0001- 5.000 mL/min(1.0 - 44 MPa), 5.0001 – 10.0000 mL/min(1.0 -22MPa)
3) Flow Rate Accuracy : ±1% (under specified condition)
4) Flow Rate Precision : Value of 0.06% RSD or 0.02 minSD, whichever greater
5) Pulsation : ≦0.08 MPa(1 mL/min, 7 MPa), ≦0.60 MPa(1 mL/min, 45 MPa)
6) Gradient mode : High-pressure gradient or Quaternary low-pressure
7) Gradient Range of Set Concentration : 0~100%(in 0.1%step)
8) Gradient Concentration Accuracy : ±0.5% (under specified condition)
9) Available pH Range : 1 - 14
10) Automatic Rinsing kit : Standard equipment
11) Degassing Unit : Connectable 1 unit
12) Auto diagnostic of the bubble detection in the flow line : possible and auto recovery(purge)
13) Flow control for the column destroying : possible and automatic setting
3. Degassing Unit(주장비)
1) Number of degassed solvents : 3
2) Max. Operating Flow rate :
3) Degassed flow line capacity : 400uL / 1 line
4) Pressure Resistance : 98kPa (1kgf/cm2) or less
4. Autosampler(주장비)
1) Injection method : Total injection(standard), loop injection(optional)
2) Injection Volume : 0.1~50uL, 0.1~2,000uL(optional)
3) Injection volume accuracy : ±1% (5μL injection, n=10)
4) Linearity : > 0.9999%
5) Injection cycle time : ≦7.8 seconds (under specified condition)
6) Samples for Processing
: 2288 (microtiter plate, 96 well × 3 plates) , 1152 (microtiter plate, 384 well × 3 plates), 252 (1 mL sample vial, 84 × 3 plates) , 162 (1.5 mL sample vial, 54 × 3 plates), 84 (4 mL sample vial, 28 × 3 plates) , 36 (10 mL sample vial, 12 × 3 plates), 72 (1.5 mL micro tube, 24 x 3 plates)
7) Injection Volume Reproducibility
: RSD≦1.0% (0.5~0.9 μL) , RSD≦0.5% (typically, 0.5 μL), RSD≦0.5% (1.0 ~1.9 μL) , RSD≦0.25% (typically, 1.0 μL), RSD≦0.25% (2.0~4.9 μL), RSD≦0.15% (5.0 μL~)
8) Carryover : <0.0005% (with rinse, typically)
9) Dip rinsing outside the needle and injection port rinsing : Standard equipment
10) Pumping rinse outside the needle : Standard equipment
11) Internal rinsing : option
12) Sample cooler : Standard equipment
13) Sample cooler temperature setting range : 4 ~ 45 ℃
14) Sample cooler temperature accuracy : ±2°C (sensor position ±0.5°C)
15) Available pH Range : 1-14
5. Column Oven(주장비)
1) Temperature control type : Forced air circulation
2) Temperature control range Room Temperature -10 ℃ ~ 100 ℃
3) Temperature accuracy : ±0.5 ℃
4) Temperature precision : 0.1 ℃
5) Containable column size and number : Up to 250 mm L. column x 6, 300 mmL. Column x 3
6. Detector(주장비)
1) UV/VIS detector
(1) Light source : Deuterium(D2) lamp
(2) Wavelength Range : 190~700 nm
(3) Bandwidth : 8nm
(4) Wavelength accuracy : ±1 nm
(5) Wavelength precision : ±0.1 nm
(6) Drift : 0.1 × 10 -3 of AU / hour or less (under specified condition)
(7) Noise : 5.0×10 -6 AU or less (under specified condition)
(8) Linearity : 2.5 AU or higher (under specified condition)
(9) Temperature coefficient : 0.1 × 10 -3 AU / ℃ or less (under specified condition)
(10) Standard Flow Cell : Optical path length :10 mm , Cell volume :12μL , Pressure :12 MPa, Material of Wetted Parts :SUS316L , PFA , quartz
(11) Cell range to set temperature : PFA , quartz
(12) Optional flow cell :
a. UHPLC cell (optical path length : 10 mm, cell volume: 8 μL, equipped with temperature control function) (Pressure 12 Mpa)
b. Semi-micro cell (optical path length: 5 mm, cell volume: 2.5 μL, equipped with temperature control function) (Pressure 12 Mpa)
c. Inert cell (optical path length: 10 mm, cell volume: 12 μL, equipped with temperature control function) (Pressure 8.0 MPa)
d. Preparative cell (optical path length : 0.1 / 0.2 / 0.5 mm, cell volume: 0.8 / 1.6 / 4.0 μL) (Pressure 3.0)
e. Micro flow cell (optical path length : 3 mm, cell volume : 0.21μL) (Pressure 8.0 MPa)
f. High maximum pressure cell (optical path length: 10 mm, cell volume: 12 μL) (Pressure 40 MPa)
(13) Available pH Range : 1-14
2) Refractive Index Detector
(1) Refractive Index measurement range : 1~1.75 RIU
(2) Noise : 2.5 × 10 -9 RIU or less
(3) Drift : 1 × 10 -7 in RIU / h or less
(4) Range : A mode:0.06 × 10-6 ~ 500 × 10-6 RIU, P, L-mode: 1 × 10 -6 to 5000 × 10 -6 RIU
(5) Response : 0.05-10 sec, 10 steps
(6) Polarity – Change : Use
(7) Zero adjustment : Auto zero, Optical Zero, Fine Zero
(8) Maximum flow rate : 20 mL / min (150 mL / min in option)
(9) Range of cell temperature control : 30 ~ 60 ℃
(10) Cell : Volume 9 μL , Maximum pressure 2 MPa
7. Data Processing Unit
1) System software
(1) HPLC System control : 4 HPLC systems can be controlled.
(2) Application : Flexibility with HPLC System Control Capability
(3) True 32-bit Software
(4) Reliable High Speed Digital Data Acquisition
(5) Comprehensive GLP/GMP Regulatory Compliance
(6) Easy Operation
(7) Automation
(8) LIMS Compatibility
(9) System suitability, Summary report, Audit trail, Security etc.
8. 악세사리(보조장비)
1) MIXER MR 180microL II (WITH CMD) 3 set
2) PIPING KIT B, for HPGE ID0.3 3 set
3) Cable ASSY for Nexera Series, D 3 set
4) Hand Tool Kit 3 set
5) MAINTENANCE KIT 3 set
6) Vial plate 1.5mL 6 set
7) Solenoid valve for drain (Teflon) 4 set
8) Power CORD SET,PHP-206S+PHS-301 2.4M (KOR) 18 set
9) LC Installaion Kit A 3 set
Include)
SafetyCap II, V2.0, GL45, 2x PFA-fitting 3,2 mm OD + air valve * 3
Solvent bottle, 1/pack * 3
Lab Total Vial Certified Kit, 100/PK
2in1 kit, 1.5ml Screw-Thread Clear Vial w/ write on spot, with cap, 100/PK
LC Column GIS C18, 5um, 4.6x150
LC Column GIS C18, 5um, 4.6x250
10) Data Processing Unit 3 set
. CPU : Intel i5
. RAM : 8GB
. HDD : 500 GB
. SSD : 128 GB
. DVD RW
. Microsoft Window 10 Professional 64 bit
. 24 inch LCD Monitor * 1 & Laser Printer